Sem/eds analysis laboratories in US in 2021
Eds testing providers by MicroVision Laboratories, Inc. in 2021? Scanning electron microscopy with energy dispersive xray spectroscopy (SEM-EDS) was used to identify the particles. The SEM showed an elevated concentration of iron and iron oxide in the impacted areas. The backscatter electron (BSE) image which correlates brightness in the image with atomic density, highlighted the iron particles that were embedded in the tile and the EDS spectrum confirms the PLM Image chemical composition of these higher density particles.
As indicated in the FTIR spectral comparison below, the suspect material showed a near perfect match for acetylsalicylic acid. Additionally, there was a small amount of dibasic phosphate present. It was determined that the material was likely acetylsalicylic acid with a phosphate binder – an aspirin. Therefore, from this analysis the suspect material in the bottle was likely a household aspirin tablet, broken apart and separated by the water. In order to confirm the identification, a few aspirin tablets from several common manufacturers were obtained, roughly ground, and soaked to allow for comparison. The optical morphology of the crystals, size range of the particles, association with the phosphate and FTIR spectrum all were consistent with the original suspect material. A report detailing the methods and findings in full narrative form was rendered to the client.
Examining the sample with a polarized light microscope (PLM), it was darker and coarser than expected for a mold sample. The dust appeared to be a closed cell, synthetic blown foam material, and all from the same source. The black color was likely due to pigment particles added to color the foam. Fourier Transform Infra-Red spectroscopy was performed on the foam particles. The spectrum showed a mixture of spectral features, associated with vinyl acetates, polyurethane, and cellulose or other sugar-like polymers. Based on these features, a common urethane acetate foam was determined as the likely source material.
MicroVision Laboratories, Inc. has been providing extensive expertise in micro-analytical techniques (FE-SEM, SEM, EDS, XRF, FTIR testing, PLM, X-Ray Imaging, DIC) and sample preparation since 2003. Our cutting edge, high-performance equipment combined with our solutions-focused customer service provide critical solutions for clients hailing from a broad range of industries ranging from medical to semiconductor, and from environmental to textile. Find a few extra info on Microvision labs sem eds analysis.
How do I submit a sample or a set of samples? To submit a sample or set of samples, please see the page How to Submit Samples. What if I believe my samples are hazardous? We are not equipped to handle or dispose of every kind of hazardous material. Please call us before sending in any potentially hazardous samples. In cases where we are able to analyze your harzardous samples we may not be able to dispose of them and therefore we will return them to you.
In Fourier Transform Infrared (FTIR) Spectroscopy samples are subjected to a broad frequency spectrum of infrared light which spans the energies of intramolecular vibrations, especially in organic compounds. The pattern and intensity of frequencies absorbed by a sample are plotted, which gives structural information about the chemical bonding state of the material. Organic compounds, which are generally very similar from an elemental standpoint, can be separated and identified using these structural fingerprints. See extra details on this website.